isolation and identification of a new phenylpropanoid derivative from the fruits of pimpinella haussknechtii rech. f. & riedl and gc-ms analysis of the essential oil
نویسندگان
چکیده
the chemical composition of the essential oil of fruits of pimpinella haussknechtiiboiss.was studied by gc-ms. after gc-ms analysis, one unknown component (56.7%) was observed, which was not characterized in the gc-ms library. the essential oil of p.hauskenekhtii was injected to hplc using ymc-pak-sil column (250 × 20 mm) with gradient system of hexane (a), and hexane: ethyl acetate, 9:1 (b) to yield the interested compound as a new phenylpropanoid derivative. its structure was elucidated as 4-(prop-2-enyl)-phenyl-3'-methylbutanoate (1) based on 13c- and 1h-nmr as well as 2d-nmr, ir and different ms spectra. in the essential oil analysis, thirty-six components, comprising 94.9% of the total oil, were identified. 4-(2-propenyl)-phenyl 3'-methylbutyrate (56.7%), bicyclogermacrene (8.9%), germacrene d (7.6%), perilla aldehyde (3.5%), and β-caryophyllene (2.9%) were found to be the major constituents of the oil. the oil of the fruits of p. haussknechtii consisted of eight monoterpene hydrocarbons (1.7%), two oxygenated monoterpenes (3.9%), sixteen sesquiterpene hydrocarbons (26.8%), two oxygenated sesquiterpenes (2.1%) and five phenylpropanoids (58.7%). three other nonterpenic compounds also comprised 1.7% of the oil.
منابع مشابه
Isolation and Identification of a New Phenylpropanoid Derivative from the Fruits of Pimpinella Haussknechtii Rech. f. & Riedl and GC-MS Analysis of the Essential Oil
The chemical composition of the essential oil of fruits of Pimpinella haussknechtiiBoiss.was studied by GC-MS. After GC-MS analysis, one unknown component (56.7%) was observed, which was not characterized in the GC-MS library. The essential oil of P.hauskenekhtii was injected to HPLC using YMC-Pak-Sil column (250 × 20 mm) with gradient system of hexane (A), and hexane: ethyl acetate, 9:1 (B) to...
متن کاملIsolation and Identification of a New Phenylpropanoid Derivative from the Fruits of Pimpinella Haussknechtii Rech. f. & Riedl and GC-MS Analysis of the Essential Oil
The chemical composition of the essential oil of fruits of Pimpinella haussknechtiiBoiss.was studied by GC-MS. After GC-MS analysis, one unknown component (56.7%) was observed, which was not characterized in the GC-MS library. The essential oil of P.hauskenekhtii was injected to HPLC using YMC-Pak-Sil column (250 × 20 mm) with gradient system of hexane (A), and hexane: ethyl acetate, 9:1 (B) to...
متن کاملIsolation and Identification of a New Phenylpropanoid Derivative from the Fruits of Pimpinella Haussknechtii Rech. f. & Riedl and GC-MS Analysis of the Essential Oil.
The chemical composition of the essential oil of fruits of Pimpinella haussknechtii. was studied by GC-MS. After GC-MS analysis, one unknown component (56.7%) was observed, which was not characterized in the GC-MS library. The essential oil of P.haussknechtii was injected to HPLC using YMC-Pak-Sil column (250 × 20 mm) with gradient system of hexane (A), and hexane: ethyl acetate, 9:1 (B) to yie...
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عنوان ژورنال:
iranian journal of pharmaceutical researchجلد ۱۴، شماره ۴، صفحات ۱۲۳۳-۱۲۳۹
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